1-Pyrrolidinecarboxylic acid, 2-(hydroxymethyl)-, 1,1-dimethylethyl ester, (2S)-, CAS No. 69610-40-8

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1-Pyrrolidinecarboxylic acid, 2-(hydroxymethyl)-, 1,1-dimethylethyl ester, (2S)- CAS No.69610-40-8 / Cat No.EBD2213716

Formula: C10H19NO3

Molecular Weight:201.26

Synonyms:

N-ALPHA-tert-Butoxycarbonyl-L-prolinol

BOC-L-Prolinol

N-Boc-L-prolinol

Boc-Pro-ol

N-(tert-Butoxycarbonyl)-L-prolinol

(S)-(-)-1-tert-Butoxycarbonyl-2-pyrrolidinemethanol

tert-butyl 2-(hydroxymethyl)pyrrolidine-1-carboxylate

tert-butyl (2S)-2-(hydroxymethyl)pyrrolidine-1-carboxylate

tert-butyl (2R)-2-(hydroxymethyl)pyrrolidine-1-carboxylate

(s)-(-)-1-boc-2-pyrrolidinemethanol

1-Pyrrolidinecarboxylic acid, 2-(hydroxymethyl)-, 1,1-dimethylethyl ester, (2S)-

2-Hydroxymethylpyrrolidine-1-carboxylic acid tert butyl ester

(S)-2-Hydroxymethyl-Pyrrolidine-1-Carboxylic Acid Tert-Butyl Ester

1-Pyrrolidinecarboxylic acid, 2-(hydroxymethyl)-, 1,1-dimethylethyl ester, (2S)-

Boc-L-prolinol

(S)-(-)-1-boc-2-pyrrolidinemethanol

n-tert-butoxycarbonyl-l-prolinol

(s)-(-)-1-(tert-butoxycarbonyl)-2-pyrrolidinemethanol

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Properties
Safety Information
NMR Spectrum

Properties

Appearance:

White powder
Density:

1.084 g/cm3
Melting point:

62-64 °C(lit.)
Boiling point:

150 °C / 4mmHg
Flashing point:

128.9 °C
Storage temperature:

Store at 0°C
Coefficient of refraction:

-55 ° (C=5, MeOH)
Optical rotation:

[α]21/D −48°, c = 1.3 in chloroform
Solubility:

insoluble

Safety Information

Symbol:
Signal words:

Warning
Hazard statements:

H315 Causes skin irritation.

H319 Causes serious eye irritation.

H335 May cause respiratory irritation.
Precautionary statements:

P261 Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.

NMR Spectrum

Prediction： H NMR (500 MHz, CDC13) delta 3.94 (dd, J = 4.9, 2.7 Hz, 2H), 3.60 (ddd, J = 18.7, 11.9, 9.3 Hz, 2H), 3.49 - 3.37 (m, 1H), 3.34 - 3.23 (m, 1H), 2.06 - 1.91 (m, 1H), 1.89 - 1.69 (m, 2H), 1.65 - 1.51 (m, 1H), 1.49 - 1.40 (m, 9H).

¹H NMR

¹³C NMR