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Di-tert-butyl Chloromethyl Phosphate CAS No.229625-50-7 / Cat No.EBD209851
Phosphoric acid, chloromethyl bis(1,1-dimethylethyl) ester
Di-tert-butyl Chloromethyl Phosphate
Properties
−20°C
Safety Information
H302 Harmful if swallowed.
H331 Toxic if inhaled.
P261 Avoid breathing dust/fume/gas/mist/vapours/spray.
P301+P312+P330 IF SWALLOWED:Call a POISON CENTER or doctor/physician if you feel unwell. Rinse mouth.
P304+P340+P312 IF INHALED:Remove victim to fresh air and keep at rest in a position comfortable for breathing. Call a POISON CENTER or doctor/physician if you feel unwell.
P403+P233 Store in a well-ventilated place. Keep container tightly closed.
NMR Spectrum
Prediction: NMR: 1H (300 MHz, CDCl3) delta 1.57 (s, 9H), 5.63 (d, 2H, J = 15 Hz). The NMR showed about 10-15percent bis-di-te/t-butyl methyl phosphate impurity that could not be removed by flash column chromatography (silica gel, ethyl acetate/hexane eluent), even with 100percent ethyl acetate eluent.
1H NMR
13C NMR